Validation of the 1H NMR Chemical Shift Method for Determination of Stereochemistry in the Bis(Tetrahydrofuranyl) Moiety of Uvaricin-Related Acetogenins from Annonaceae: Rolliniastatin 1 (and Asimicin)

Thomas R. Hoye; Zhi ping Zhuang

doi:10.1021/jo00258a045

Validation of the ¹H NMR Chemical Shift Method for Determination of Stereochemistry in the Bis(Tetrahydrofuranyl) Moiety of Uvaricin-Related Acetogenins from Annonaceae: Rolliniastatin 1 (and Asimicin)

Thomas R. Hoye
, Zhi ping Zhuang

Chemistry (Twin Cities)

Research output: Contribution to journal › Article › peer-review

84 Scopus citations

Abstract

A valuable new method for quantitative correlation of the ¹H NMR chemical shift data from the appropriate members (a, g) of a set of model diastereomeric bis(tetrahydrofurans) (2a-l) with those from the triacetate derivative of rolliniastatin 1 (5) was developed.

Original language	English (US)
Pages (from-to)	5578-5580
Number of pages	3
Journal	Journal of Organic Chemistry
Volume	53
Issue number	23
DOIs	https://doi.org/10.1021/jo00258a045
State	Published - Nov 1 1988

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10.1021/jo00258a045

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Validation of the ¹H NMR Chemical Shift Method for Determination of Stereochemistry in the Bis(Tetrahydrofuranyl) Moiety of Uvaricin-Related Acetogenins from Annonaceae: Rolliniastatin 1 (and Asimicin). / Hoye, Thomas R.; Zhuang, Zhi ping.
In: Journal of Organic Chemistry, Vol. 53, No. 23, 01.11.1988, p. 5578-5580.

Research output: Contribution to journal › Article › peer-review

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abstract = "A valuable new method for quantitative correlation of the 1H NMR chemical shift data from the appropriate members (a, g) of a set of model diastereomeric bis(tetrahydrofurans) (2a-l) with those from the triacetate derivative of rolliniastatin 1 (5) was developed.",

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Validation of the ¹H NMR Chemical Shift Method for Determination of Stereochemistry in the Bis(Tetrahydrofuranyl) Moiety of Uvaricin-Related Acetogenins from Annonaceae: Rolliniastatin 1 (and Asimicin)

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