Synthesis of multiwall α-Fe                         
                        2
                                                 O                         
                        3
                                                  hollow fibers via a centrifugal spinning technique

Mandana Akia; Andre Mkhoyan; Karen Lozano

doi:10.1016/j.msec.2019.04.085

Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique

Mandana Akia, Andre Mkhoyan, Karen Lozano

Research output: Contribution to journal › Article › peer-review

35 Scopus citations

Abstract

Hollow hematite (α-Fe₂O₃) fine fibers with multiwall structure were synthesized by utilizing a centrifugal spinning technique. Aqueous solutions of polyvinyl pyrrolidone and iron (III) nitrate nonahydrate were prepared and spun into fibers. The precursor fibers were heat treated at 650 °C to form iron oxide fibers. Scanning electron micrographs revealed the formation of iron oxide hollow fibers with multiwall structure with average wall thickness of 55 ± 15 nm and outer fiber diameter of 852 ± 86 nm. The formation of α-Fe₂O₃ was confirmed by X-ray diffraction analysis and the phase identification was verified by XRD pattern and transmission electron microscopy analysis. These hollow structure α-Fe₂O₃ fibers have promising uses in important biological processes and biomedical applications.

Original language	English (US)
Pages (from-to)	552-557
Number of pages	6
Journal	Materials Science and Engineering C
Volume	102
DOIs	https://doi.org/10.1016/j.msec.2019.04.085
State	Published - Sep 2019

Bibliographical note

Funding Information:
This research was supported by NSF PREM award under grant No. DMR-1523577: UTRGV-UMN Partnership for Fostering Innovation by Bridging Excellence in Research and Student Success. This project was partially supported by the MRSEC program of the National Science Foundation under Award DMR-1420013. STEM analysis was performed in the College of Science and Engineering Characterization Facility of the University of Minnesota, which receives partial support from the NSF through the MRSEC program. We also like to thank Dr. Jason Myers and Mr. Jacob Held for their assistance with STEM data acquisition.

Funding Information:
This research was supported by NSF PREM award under grant No. DMR-1523577 : UTRGV-UMN Partnership for Fostering Innovation by Bridging Excellence in Research and Student Success. This project was partially supported by the MRSEC program of the National Science Foundation under Award DMR-1420013 . STEM analysis was performed in the College of Science and Engineering Characterization Facility of the University of Minnesota, which receives partial support from the NSF through the MRSEC program. We also like to thank Dr. Jason Myers and Mr. Jacob Held for their assistance with STEM data acquisition.

Publisher Copyright:
© 2019 Elsevier B.V.

Keywords

Centrifugal spinning
Composite
Hollow fibers
Multiwall
α-Fe O

MRSEC Support

Partial

PubMed: MeSH publication types

Journal Article

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10.1016/j.msec.2019.04.085

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Cite this

Akia, M., Mkhoyan, A., & Lozano, K. (2019). Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique. Materials Science and Engineering C, 102, 552-557. https://doi.org/10.1016/j.msec.2019.04.085

Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique. / Akia, Mandana; Mkhoyan, Andre; Lozano, Karen.
In: Materials Science and Engineering C, Vol. 102, 09.2019, p. 552-557.

Research output: Contribution to journal › Article › peer-review

Akia, M, Mkhoyan, A & Lozano, K 2019, 'Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique', Materials Science and Engineering C, vol. 102, pp. 552-557. https://doi.org/10.1016/j.msec.2019.04.085

Akia M, Mkhoyan A, Lozano K. Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique. Materials Science and Engineering C. 2019 Sep;102:552-557. doi: 10.1016/j.msec.2019.04.085

Akia, Mandana ; Mkhoyan, Andre ; Lozano, Karen. / Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique. In: Materials Science and Engineering C. 2019 ; Vol. 102. pp. 552-557.

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abstract = "Hollow hematite (α-Fe2O3) fine fibers with multiwall structure were synthesized by utilizing a centrifugal spinning technique. Aqueous solutions of polyvinyl pyrrolidone and iron (III) nitrate nonahydrate were prepared and spun into fibers. The precursor fibers were heat treated at 650 °C to form iron oxide fibers. Scanning electron micrographs revealed the formation of iron oxide hollow fibers with multiwall structure with average wall thickness of 55 ± 15 nm and outer fiber diameter of 852 ± 86 nm. The formation of α-Fe2O3 was confirmed by X-ray diffraction analysis and the phase identification was verified by XRD pattern and transmission electron microscopy analysis. These hollow structure α-Fe2O3 fibers have promising uses in important biological processes and biomedical applications.",

keywords = "Centrifugal spinning, Composite, Hollow fibers, Multiwall, α-Fe O",

author = "Mandana Akia and Andre Mkhoyan and Karen Lozano",

note = "Funding Information: This research was supported by NSF PREM award under grant No. DMR-1523577: UTRGV-UMN Partnership for Fostering Innovation by Bridging Excellence in Research and Student Success. This project was partially supported by the MRSEC program of the National Science Foundation under Award DMR-1420013. STEM analysis was performed in the College of Science and Engineering Characterization Facility of the University of Minnesota, which receives partial support from the NSF through the MRSEC program. We also like to thank Dr. Jason Myers and Mr. Jacob Held for their assistance with STEM data acquisition. Funding Information: This research was supported by NSF PREM award under grant No. DMR-1523577 : UTRGV-UMN Partnership for Fostering Innovation by Bridging Excellence in Research and Student Success. This project was partially supported by the MRSEC program of the National Science Foundation under Award DMR-1420013 . STEM analysis was performed in the College of Science and Engineering Characterization Facility of the University of Minnesota, which receives partial support from the NSF through the MRSEC program. We also like to thank Dr. Jason Myers and Mr. Jacob Held for their assistance with STEM data acquisition. Publisher Copyright: {\textcopyright} 2019 Elsevier B.V.",

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N2 - Hollow hematite (α-Fe2O3) fine fibers with multiwall structure were synthesized by utilizing a centrifugal spinning technique. Aqueous solutions of polyvinyl pyrrolidone and iron (III) nitrate nonahydrate were prepared and spun into fibers. The precursor fibers were heat treated at 650 °C to form iron oxide fibers. Scanning electron micrographs revealed the formation of iron oxide hollow fibers with multiwall structure with average wall thickness of 55 ± 15 nm and outer fiber diameter of 852 ± 86 nm. The formation of α-Fe2O3 was confirmed by X-ray diffraction analysis and the phase identification was verified by XRD pattern and transmission electron microscopy analysis. These hollow structure α-Fe2O3 fibers have promising uses in important biological processes and biomedical applications.

AB - Hollow hematite (α-Fe2O3) fine fibers with multiwall structure were synthesized by utilizing a centrifugal spinning technique. Aqueous solutions of polyvinyl pyrrolidone and iron (III) nitrate nonahydrate were prepared and spun into fibers. The precursor fibers were heat treated at 650 °C to form iron oxide fibers. Scanning electron micrographs revealed the formation of iron oxide hollow fibers with multiwall structure with average wall thickness of 55 ± 15 nm and outer fiber diameter of 852 ± 86 nm. The formation of α-Fe2O3 was confirmed by X-ray diffraction analysis and the phase identification was verified by XRD pattern and transmission electron microscopy analysis. These hollow structure α-Fe2O3 fibers have promising uses in important biological processes and biomedical applications.

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Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique

Abstract

Bibliographical note

Keywords

MRSEC Support

PubMed: MeSH publication types

Publisher link

Find It

Other files and links

Fingerprint

Partnership for Research and Education in Materials

MRSEC IRG-2: Sustainable Nanocrystal Materials

University of Minnesota MRSEC (DMR-1420013)

Cite this

Synthesis of multiwall α-Fe 2 O 3 hollow fibers via a centrifugal spinning technique

Abstract

Bibliographical note

Keywords

MRSEC Support

PubMed: MeSH publication types

Publisher link

Find It

Other files and links

Fingerprint

Projects

Partnership for Research and Education in Materials

MRSEC IRG-2: Sustainable Nanocrystal Materials

University of Minnesota MRSEC (DMR-1420013)

Cite this

Synthesis of multiwall α-Fe ₂ O ₃ hollow fibers via a centrifugal spinning technique