Synthesis and X-Ray Structure Determination of 1,4-Bis[trimethylsilylethynyl(trifluoromethanesulfonyloxy)iodo]benzene, Me3SiC≡Cl+C6H4l+C≡CSiMe3 2CF3SO3−, a Novel Alkynyliodonium Salt

Peter J. Stang; Viktor V. Zhdankin; Atta M. Arif

doi:10.1070/MC1992v002n04ABEH000184

Synthesis and X-Ray Structure Determination of 1,4-Bis[trimethylsilylethynyl(trifluoromethanesulfonyloxy)iodo]benzene, Me₃SiC≡Cl⁺C₆H₄l⁺C≡CSiMe₃ 2CF₃SO₃⁻, a Novel Alkynyliodonium Salt

Peter J. Stang
, Viktor V. Zhdankin
, Atta M. Arif

Chemistry & Biochemistry

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

The novel bis(alkynyliodonium) salt, 2, has been prepared by the reaction of p-bis(iodosyl)benzene with trimethylsilyl trifluoromethanesulfonate and bis(trimethylsilyl)acetylene; X-ray structure analysis reveals an unusual basket-like structure for this compound.

Original language	English (US)
Pages (from-to)	158-159
Number of pages	2
Journal	Mendeleev Communications
Volume	2
Issue number	4
DOIs	https://doi.org/10.1070/MC1992v002n04ABEH000184
State	Published - Jan 1 1992

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10.1070/MC1992v002n04ABEH000184

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Synthesis and X-Ray Structure Determination of 1,4-Bis[trimethylsilylethynyl(trifluoromethanesulfonyloxy)iodo]benzene, Me₃SiC≡Cl⁺C₆H₄l⁺C≡CSiMe₃ 2CF₃SO₃⁻, a Novel Alkynyliodonium Salt. / Stang, Peter J.; Zhdankin, Viktor V.; Arif, Atta M.
In: Mendeleev Communications, Vol. 2, No. 4, 01.01.1992, p. 158-159.

Research output: Contribution to journal › Article › peer-review

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abstract = "The novel bis(alkynyliodonium) salt, 2, has been prepared by the reaction of p-bis(iodosyl)benzene with trimethylsilyl trifluoromethanesulfonate and bis(trimethylsilyl)acetylene; X-ray structure analysis reveals an unusual basket-like structure for this compound.",

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AB - The novel bis(alkynyliodonium) salt, 2, has been prepared by the reaction of p-bis(iodosyl)benzene with trimethylsilyl trifluoromethanesulfonate and bis(trimethylsilyl)acetylene; X-ray structure analysis reveals an unusual basket-like structure for this compound.

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Synthesis and X-Ray Structure Determination of 1,4-Bis[trimethylsilylethynyl(trifluoromethanesulfonyloxy)iodo]benzene, Me₃SiC≡Cl⁺C₆H₄l⁺C≡CSiMe₃ 2CF₃SO₃⁻, a Novel Alkynyliodonium Salt

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