[18O]‐Chlorocarbonylsulfenyl chloride with an isotopic purity of 92% was prepared in three steps starting with the [18O]‐hydrolysis of 2‐ethyl‐1,3‐dioxolane to [18O]‐propanal, which was then converted to [18O]‐O‐1‐methylpropyl S‐methyl dithiocarbonate, which was then chlorinated to give the title compound. Distilled yields for the three steps were 57%, 49%, and 40% respectively.
|Original language||English (US)|
|Number of pages||8|
|Journal||Journal of Labelled Compounds and Radiopharmaceuticals|
|State||Published - Apr 1984|
- [O]‐chlorocarbonylsulfenyl chloride