Preparation and chemistry of 1-organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones: First example of a stable adduct of 2-iodosobenzoic acid with strong acid

Viktor Zhdankin; Chris J. Kuehl; Jason T. Bolz; Mark S. Formaneck; Angela J. Simonsen

doi:10.1016/0040-4039(94)85304-5

Preparation and chemistry of 1-organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones: First example of a stable adduct of 2-iodosobenzoic acid with strong acid

Viktor Zhdankin, Chris J. Kuehl, Jason T. Bolz, Mark S. Formaneck, Angela J. Simonsen

Chemistry & Biochemistry

Research output: Contribution to journal › Article › peer-review

32 Scopus citations

Abstract

1-Organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones (3,4,5) can be prepared in one step from 2-iodosobenzoic acid and the corresponding sulfonic acids or Me₃SiOTf. Reactions of these compounds with bis(trimethylsilyl)acetylene or cyanotrimethylsilane afford the respective alkynyl or cyano iodonium salts 6, 7, 8.

Original language	English (US)
Pages (from-to)	7323-7326
Number of pages	4
Journal	Tetrahedron Letters
Volume	35
Issue number	40
DOIs	https://doi.org/10.1016/0040-4039(94)85304-5
State	Published - Oct 3 1994

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title = "Preparation and chemistry of 1-organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones: First example of a stable adduct of 2-iodosobenzoic acid with strong acid",

abstract = "1-Organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones (3,4,5) can be prepared in one step from 2-iodosobenzoic acid and the corresponding sulfonic acids or Me3SiOTf. Reactions of these compounds with bis(trimethylsilyl)acetylene or cyanotrimethylsilane afford the respective alkynyl or cyano iodonium salts 6, 7, 8.",

author = "Viktor Zhdankin and Kuehl, {Chris J.} and Bolz, {Jason T.} and Formaneck, {Mark S.} and Simonsen, {Angela J.}",

year = "1994",

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doi = "10.1016/0040-4039(94)85304-5",

language = "English (US)",

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journal = "Tetrahedron Letters",

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T1 - Preparation and chemistry of 1-organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones

T2 - First example of a stable adduct of 2-iodosobenzoic acid with strong acid

AU - Zhdankin, Viktor

AU - Kuehl, Chris J.

AU - Bolz, Jason T.

AU - Formaneck, Mark S.

AU - Simonsen, Angela J.

PY - 1994/10/3

Y1 - 1994/10/3

N2 - 1-Organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones (3,4,5) can be prepared in one step from 2-iodosobenzoic acid and the corresponding sulfonic acids or Me3SiOTf. Reactions of these compounds with bis(trimethylsilyl)acetylene or cyanotrimethylsilane afford the respective alkynyl or cyano iodonium salts 6, 7, 8.

AB - 1-Organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones (3,4,5) can be prepared in one step from 2-iodosobenzoic acid and the corresponding sulfonic acids or Me3SiOTf. Reactions of these compounds with bis(trimethylsilyl)acetylene or cyanotrimethylsilane afford the respective alkynyl or cyano iodonium salts 6, 7, 8.

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U2 - 10.1016/0040-4039(94)85304-5

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VL - 35

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EP - 7326

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 40

ER -

Preparation and chemistry of 1-organosulfonyloxy-1,2-benziodoxol-3-(1H)-ones: First example of a stable adduct of 2-iodosobenzoic acid with strong acid

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