Optimization of a process for carboxymethyl cellulose (CMC) preparation in mixed solvents

Hua Zhao, Fa Cheng, Guifeng Li, Jingwu Zhang

Research output: Contribution to journalArticlepeer-review

21 Scopus citations

Abstract

A benzene - ethanol - water mixture was investigated as the solvent medium in synthesizing carboxymethyl cellulose (CMC). The process of carboxymethylation was optimized to produce CMC with DS > I.0, solution viscosity about 1500 mpa·s, and with uniform distribution of substituents. It is possible to scale up this process by using a kneading machine.

Original languageEnglish (US)
Pages (from-to)749-759
Number of pages11
JournalInternational Journal of Polymeric Materials and Polymeric Biomaterials
Volume52
Issue number9
DOIs
StatePublished - Sep 2003
Externally publishedYes

Keywords

  • Carboxymethyl cellulose (CMC)
  • Degree of substitution (DS)
  • Uniform substituants

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