One-pot synthesis of diaryliodonium salts from arenes and aryl iodides with Oxone-sulfuric acid

Natalia Soldatova, Pavel Postnikov, Olga Kukurina, Viktor V. Zhdankin, Akira Yoshimura, Thomas Wirth, Mekhman S. Yusubov

Research output: Contribution to journalArticle

5 Scopus citations

Abstract

A facile synthesis of diaryliodonium salts utilizing Oxone as versatile and cheap oxidant has been developed. This method shows wide applicability and can be used for the preparation of iodonium salts containing electron-donating or electron-withdrawing groups in good yields. In addition, this procedure can be applied to the preparation of symmetric iodonium salts directly from arenes via a one-pot iodination-oxidation sequence.

Original languageEnglish (US)
Pages (from-to)849-855
Number of pages7
JournalBeilstein Journal of Organic Chemistry
Volume14
DOIs
StatePublished - Apr 12 2018

Keywords

  • Diaryliodonium salts
  • Iodine
  • Iodonium
  • Oxidation
  • Oxone

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