Microwave-assisted synthesis of highly crystalline mesoporous hydroxyapatite with a Rod-shaped morphology

Mercy R. Benzigar; Gurudas P. Mane; Siddulu N. Talapaneni; Shaji Varghese; Chokkalingam Anand; Salem S. Aldeyab; Veerappan V. Balasubramanian; Ajayan Vinu

doi:10.1246/cl.2012.458

Microwave-assisted synthesis of highly crystalline mesoporous hydroxyapatite with a Rod-shaped morphology

Mercy R. Benzigar, Gurudas P. Mane, Siddulu N. Talapaneni, Shaji Varghese, Chokkalingam Anand, Salem S. Aldeyab, Veerappan V. Balasubramanian, Ajayan Vinu

Chemical Engineering and Materials Science

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl ₂ and K ₂HPO ₄ as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120°C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.

Original language	English (US)
Pages (from-to)	458-460
Number of pages	3
Journal	Chemistry Letters
Volume	41
Issue number	4
DOIs	https://doi.org/10.1246/cl.2012.458
State	Published - 2012

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10.1246/cl.2012.458

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title = "Microwave-assisted synthesis of highly crystalline mesoporous hydroxyapatite with a Rod-shaped morphology",

abstract = "Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl 2 and K 2HPO 4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120°C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.",

author = "Benzigar, {Mercy R.} and Mane, {Gurudas P.} and Talapaneni, {Siddulu N.} and Shaji Varghese and Chokkalingam Anand and Aldeyab, {Salem S.} and Balasubramanian, {Veerappan V.} and Ajayan Vinu",

year = "2012",

doi = "10.1246/cl.2012.458",

language = "English (US)",

volume = "41",

pages = "458--460",

journal = "Chemistry Letters",

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T1 - Microwave-assisted synthesis of highly crystalline mesoporous hydroxyapatite with a Rod-shaped morphology

AU - Benzigar, Mercy R.

AU - Mane, Gurudas P.

AU - Talapaneni, Siddulu N.

AU - Varghese, Shaji

AU - Anand, Chokkalingam

AU - Aldeyab, Salem S.

AU - Balasubramanian, Veerappan V.

AU - Vinu, Ajayan

PY - 2012

Y1 - 2012

N2 - Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl 2 and K 2HPO 4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120°C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.

AB - Mesoporous hydroxyapatite (MHA) with a rod-shaped morphology has been successfully synthesized for the first time employing cetyltrimethylammonium bromide (CTAB) as a template and CaCl 2 and K 2HPO 4 as the precursors for hydroxyapatite under alkaline medium at the reaction temperature of 120°C via microwave method. The obtained material exhibits a disordered mesoporous structure with a high crystallinity and highly uniform rod-like morphology with an average size of ca. 25 nm in width and 100 nm in length.

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U2 - 10.1246/cl.2012.458

DO - 10.1246/cl.2012.458

M3 - Article

AN - SCOPUS:84859905514

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VL - 41

SP - 458

EP - 460

JO - Chemistry Letters

JF - Chemistry Letters

IS - 4

ER -

Microwave-assisted synthesis of highly crystalline mesoporous hydroxyapatite with a Rod-shaped morphology

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