Improved synthesis of various isotope labeled 4-hydroxyalkenals and peroxidation intermediates

M. S. Rees, F. J.G.M. van Kuijk, A. N. Siakotos, B. P. Mundy

Research output: Contribution to journalArticlepeer-review

25 Scopus citations

Abstract

A concise and isotope specific synthesis of perfluorobenzyl 5,5,6,6-tetradeutero-9-oxononanoate and an abbreviated general multi-isotope synthesis of 4-hydroxyalkenals is reported.

Original languageEnglish (US)
Pages (from-to)3225-3236
Number of pages12
JournalSynthetic Communications
Volume25
Issue number20
DOIs
StatePublished - Oct 1 1995

Bibliographical note

Funding Information:
FJGMvK was supported by the Air Force Office of Scientific Research, Air Force Systems Command, USAF, under grant #90-0327 and #93-NL036. The U.S. government is authorized to reproduce and distribute reprints for governmental purposes notwithstanding any copyright notation hereon. ANS was supported by the NIH under grant #NS-30171 and by the Children’s Brain Disease Foundation. The authors thank L. Joe Sears for assistance with the high resolution mass spectrometry.

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