@inproceedings{9dafd627453c4a1299386985e9ffb94b,
title = "Evolution of sol-gel films in the environmental scanning electron microscope",
abstract = "The ability to study the surface texture of a sol-gel film of lead titanate as it is heated in-situ in an environmental scanning electron microscope is demonstrated. Measurements of the shrinkage of the film at cracks and around delaminations of several microns have been made. Grain sizes of the final crystalline microstructure were determined to be approx. 0.2 μm. The formation of bumps in the film 1-5 μm in size was observed. The presence of these features may correlate with the onset of crystallization.",
author = "Stuart McKernan and John Wright and Francis, {Lorraine F}",
year = "1994",
month = jan,
day = "1",
language = "English (US)",
isbn = "1558992200",
series = "Materials Research Society Symposium Proceedings",
publisher = "Publ by Materials Research Society",
pages = "561--566",
editor = "Matthew Libera and Haynes, {Tony E.} and Peggy Cebe and {Dickinson Jr.}, {James E.}",
booktitle = "Crystallization and Related Phenomena in Amorphous Materials",
note = "Proceedings of the 1993 Fall Meeting of the Materials Research Society ; Conference date: 29-11-1993 Through 02-12-1993",
}