Evaluation of the physical and chemical properties of two commercial and three experimental root-end filling materials

Rodrigo Ricci Vivan, Ronald Ordinola Zapata, Mrcia A. Zeferino, Clovis Monteiro Bramante, Norberti Bernardineli, Roberto Brando Garcia, Marco Antonio Hungaro Duarte, Mrio Tanomaru Filho, Ivaldo Gomes De Moraes

Research output: Contribution to journalArticlepeer-review

69 Scopus citations

Abstract

Objective: The aim of this study was to evaluate the pH, calcium release, setting time, and solubility of two commercially available mineral trioxide aggregate (MTA) cements (white MTA Angelus and MTA Bio), and of three experimental cements (light-cured MTA, Portland cement with 20% bismuth oxide and 5% calcium sulfate, and an epoxy resinbased cement). Study design: For evaluation of pH and calcium ion release, polyethylene tubes with 1.0 mm internal diameter and 10.0 mm length were filled with the cements and immediately immersed in flasks containing 10 mL deionized water. After 3, 24, 72, and 168 hours, the tubes were removed and the water from the previous container was measured for its pH and calcium content with a pH meter and an atomic absorption spectrophotometer. For analysis of the setting time, Gilmore needles weighing 100 g and 456.5 g were used, in accordance with the American Society for Testing and Materials specification no. C266-03. Solubility of each cement was also tested. Results: All the cements were alkaline and released calcium ions, with a declining trend over time. After 3 hours, Portland cement + bismuth oxide and MTA Bio had the highest pH and light-cured MTA the lowest. After 1 week, MTA Bio had the highest pH and light-cured MTA and epoxy resinbased cement the lowest. Regarding calcium ion release, after 3 hours, Portland cement + bismuth oxide showed the highest release. After 1 week, MTA Bio had the highest. Epoxy resinbased cement and light-cured MTA had the lowest calcium release in all evaluation periods. Regarding setting times, white MTA Angelus and MTA Bio had the shortest, Portland cement + bismuth oxide had an intermediate setting time, and the epoxy resinbased cement had the longest. The materials that showed the lowest solubility values were the epoxy resinbased cement, Portland cement + bismuth oxide, and light-cured MTA. The highest solubility values were presented in white MTA Angelus and MTA Bio. Conclusions: The white MTA Angelus and MTA Bio had the shortest setting times, higher pH and calcium ion release, and the highest solubility. In contrast, the epoxy resinbased cement and light-cured MTA showed lower values of solubility, pH, and calcium ion release.

Original languageEnglish (US)
Pages (from-to)250-256
Number of pages7
JournalOral Surgery, Oral Medicine, Oral Pathology, Oral Radiology and Endodontology
Volume110
Issue number2
DOIs
StatePublished - Aug 13 2010
Externally publishedYes

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