Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

Jason A. Halfen, Victor G. Young

Research output: Contribution to journalArticlepeer-review

22 Scopus citations

Abstract

A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

Original languageEnglish (US)
Pages (from-to)2894-2895
Number of pages2
JournalChemical Communications
Volume3
Issue number23
DOIs
StatePublished - Jan 1 2003

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