Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

Jason A. Halfen; Victor G. Young

doi:10.1039/b311520h

Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

Jason A. Halfen, Victor G. Young

Chemistry (Twin Cities)

Research output: Contribution to journal › Article › peer-review

22 Scopus citations

Abstract

A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

Original language	English (US)
Pages (from-to)	2894-2895
Number of pages	2
Journal	Chemical Communications
Volume	3
Issue number	23
DOIs	https://doi.org/10.1039/b311520h
State	Published - Jan 1 2003

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title = "Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate",

abstract = "A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.",

author = "Halfen, {Jason A.} and Young, {Victor G.}",

year = "2003",

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doi = "10.1039/b311520h",

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N2 - A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

AB - A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

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