Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

Jason A. Halfen; Victor G. Young

doi:10.1039/b311520h

Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

Jason A. Halfen, Victor G. Young

Chemistry (Twin Cities)

Research output: Contribution to journal › Article › peer-review

23 Scopus citations

Abstract

A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

Original language	English (US)
Pages (from-to)	2894-2895
Number of pages	2
Journal	Chemical Communications
Volume	3
Issue number	23
DOIs	https://doi.org/10.1039/b311520h
State	Published - 2003

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title = "Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate",

abstract = "A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.",

author = "Halfen, {Jason A.} and Young, {Victor G.}",

year = "2003",

doi = "10.1039/b311520h",

language = "English (US)",

volume = "3",

pages = "2894--2895",

journal = "Chemical Communications",

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publisher = "Royal Society of Chemistry",

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T1 - Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

AU - Halfen, Jason A.

AU - Young, Victor G.

PY - 2003

Y1 - 2003

N2 - A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

AB - A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(ii) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.

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U2 - 10.1039/b311520h

DO - 10.1039/b311520h

M3 - Article

AN - SCOPUS:0345305303

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EP - 2895

JO - Chemical Communications

JF - Chemical Communications

SN - 1359-7345

IS - 23

ER -

Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

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