Dual acquisition magic-angle spinning solid-State NMR-spectroscopy: Simultaneous acquisition of multidimensional spectra of biomacromolecules

T. Gopinath, Gianluigi Veglia

Research output: Contribution to journalArticlepeer-review

59 Scopus citations

Abstract

Fast data collection: A general method for dual data acquisition of multidimensional magic-angle spinning solid-state NMR experiments is presented (see picture). The method uses a simultaneous Hartmann-Hahn cross-polarization from 1H to 13C and 15N nuclei and exploits the long-living 15N polarization for parallel acquisition of two multidimensional experiments.

Original languageEnglish (US)
Pages (from-to)2731-2735
Number of pages5
JournalAngewandte Chemie - International Edition
Volume51
Issue number11
DOIs
StatePublished - Mar 12 2012

Keywords

  • NMR spectroscopy
  • magic-angle spinning
  • proteins
  • solid-state structures
  • structure elucidation

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