TY - JOUR
T1 - Bis(N-methyl-N-phenylcarbamoyl)-disulfane
AU - Schroll, Alayne L.
AU - Pink, Maren
AU - Barany, George
PY - 2012/5
Y1 - 2012/5
N2 - The title compound, C16H16N2O 2S2, has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago. We now confirm the proposed molecular structure in which the molecule exhibits a twofold axis of symmetry through the mid-point of the S - S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].
AB - The title compound, C16H16N2O 2S2, has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago. We now confirm the proposed molecular structure in which the molecule exhibits a twofold axis of symmetry through the mid-point of the S - S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].
UR - https://www.scopus.com/pages/publications/84860770687
UR - https://www.scopus.com/pages/publications/84860770687#tab=citedBy
U2 - 10.1107/S1600536812016030
DO - 10.1107/S1600536812016030
M3 - Article
C2 - 22590411
AN - SCOPUS:84860770687
SN - 1600-5368
VL - 68
SP - o1550
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 5
ER -