Activation of giant silicalite-1 monocrystals combining rapid thermal processing and ozone calcination

Marta Navarro; Ester Mateo; Beatriz Diosdado; Michael Tsapatsis; Joaquín Coronas

doi:10.1039/c4ra16284f

Activation of giant silicalite-1 monocrystals combining rapid thermal processing and ozone calcination

Marta Navarro
, Ester Mateo
, Beatriz Diosdado
, Michael Tsapatsis
, Joaquín Coronas

Chemical Engineering and Materials Science

Research output: Contribution to journal › Article › peer-review

7 Scopus citations

Abstract

A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm² section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent.

Original language	English (US)
Pages (from-to)	18035-18040
Number of pages	6
Journal	RSC Advances
Volume	5
Issue number	23
DOIs	https://doi.org/10.1039/c4ra16284f
State	Published - 2015

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© 2015 The Royal Society of Chemistry.

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10.1039/c4ra16284f

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abstract = "A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm2 section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent.",

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AU - Mateo, Ester

AU - Diosdado, Beatriz

AU - Tsapatsis, Michael

AU - Coronas, Joaquín

PY - 2015

Y1 - 2015

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AB - A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm2 section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent.

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UR - https://www.scopus.com/pages/publications/84923169493#tab=citedBy

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DO - 10.1039/c4ra16284f

M3 - Article

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JO - RSC Advances

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ER -

Activation of giant silicalite-1 monocrystals combining rapid thermal processing and ozone calcination

Abstract

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