A general approach to unsymmetrical tricoordinate iodinanes: Single step preparation of mixed iodosobenzene sulfonates Phl(X)OSO2R, via reaction of iodosobenzene with Me3SiX

Viktor V. Zhdankin; Charles M. Crittell; Peter J. Stang; Nikolai S. Zefirov

doi:10.1016/S0040-4039(00)97741-4

A general approach to unsymmetrical tricoordinate iodinanes: Single step preparation of mixed iodosobenzene sulfonates Phl(X)OSO₂R, via reaction of iodosobenzene with Me₃SiX

Viktor V. Zhdankin, Charles M. Crittell, Peter J. Stang, Nikolai S. Zefirov

Chemistry & Biochemistry

Research output: Contribution to journal › Article › peer-review

66 Scopus citations

Abstract

Mixed iodonium sulfonates of the type Phl(X)OSO₂R (X = OAc, NHAc, NCO, CN; R = CF₃, C₄F₉, p-CH₃C₆H₄) have been prepared by the reaction of PhlO with the appropriate derivatives of trimethylsilane.

Original language	English (US)
Pages (from-to)	4821-4824
Number of pages	4
Journal	Tetrahedron Letters
Volume	31
Issue number	34
DOIs	https://doi.org/10.1016/S0040-4039(00)97741-4
State	Published - 1990

Bibliographical note

Funding Information:
6 7 8 This reaction is similar to the one with [hydroxy(sulfonyloxy)iodo]benzene resulting in a-sulfonyloxy carbonyl compounds5. F. This work was supported by the NCI of NIH (2ROCA16903) in the USA.

Copyright:
Copyright 2014 Elsevier B.V., All rights reserved.

Publisher link

10.1016/S0040-4039(00)97741-4

Find It

Find It at U of M Libraries

Cite this

A general approach to unsymmetrical tricoordinate iodinanes: Single step preparation of mixed iodosobenzene sulfonates Phl(X)OSO₂R, via reaction of iodosobenzene with Me₃SiX. / Zhdankin, Viktor V.; Crittell, Charles M.; Stang, Peter J. et al.
In: Tetrahedron Letters, Vol. 31, No. 34, 1990, p. 4821-4824.

Research output: Contribution to journal › Article › peer-review

@article{e357fa14fc9f46c39f4ca0b5bc64f05e,

title = "A general approach to unsymmetrical tricoordinate iodinanes: Single step preparation of mixed iodosobenzene sulfonates Phl(X)OSO2R, via reaction of iodosobenzene with Me3SiX",

abstract = "Mixed iodonium sulfonates of the type Phl(X)OSO2R (X = OAc, NHAc, NCO, CN; R = CF3, C4F9, p-CH3C6H4) have been prepared by the reaction of PhlO with the appropriate derivatives of trimethylsilane.",

author = "Zhdankin, {Viktor V.} and Crittell, {Charles M.} and Stang, {Peter J.} and Zefirov, {Nikolai S.}",

note = "Funding Information: 6 7 8 This reaction is similar to the one with [hydroxy(sulfonyloxy)iodo]benzene resulting in a-sulfonyloxy carbonyl compounds5. F. This work was supported by the NCI of NIH (2ROCA16903) in the USA. Copyright: Copyright 2014 Elsevier B.V., All rights reserved.",

year = "1990",

doi = "10.1016/S0040-4039(00)97741-4",

language = "English (US)",

volume = "31",

pages = "4821--4824",

journal = "Tetrahedron Letters",

issn = "0040-4039",

publisher = "Elsevier Limited",

number = "34",

}

TY - JOUR

T1 - A general approach to unsymmetrical tricoordinate iodinanes

T2 - Single step preparation of mixed iodosobenzene sulfonates Phl(X)OSO2R, via reaction of iodosobenzene with Me3SiX

AU - Zhdankin, Viktor V.

AU - Crittell, Charles M.

AU - Stang, Peter J.

AU - Zefirov, Nikolai S.

N1 - Funding Information: 6 7 8 This reaction is similar to the one with [hydroxy(sulfonyloxy)iodo]benzene resulting in a-sulfonyloxy carbonyl compounds5. F. This work was supported by the NCI of NIH (2ROCA16903) in the USA. Copyright: Copyright 2014 Elsevier B.V., All rights reserved.

PY - 1990

Y1 - 1990

N2 - Mixed iodonium sulfonates of the type Phl(X)OSO2R (X = OAc, NHAc, NCO, CN; R = CF3, C4F9, p-CH3C6H4) have been prepared by the reaction of PhlO with the appropriate derivatives of trimethylsilane.

AB - Mixed iodonium sulfonates of the type Phl(X)OSO2R (X = OAc, NHAc, NCO, CN; R = CF3, C4F9, p-CH3C6H4) have been prepared by the reaction of PhlO with the appropriate derivatives of trimethylsilane.

UR - http://www.scopus.com/inward/record.url?scp=0025005096&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0025005096&partnerID=8YFLogxK

U2 - 10.1016/S0040-4039(00)97741-4

DO - 10.1016/S0040-4039(00)97741-4

M3 - Article

AN - SCOPUS:0025005096

SN - 0040-4039

VL - 31

SP - 4821

EP - 4824

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 34

ER -