A facile hydrothermal synthesis route to single-crystalline lead iodide nanobelts and nanobelt bundles

Dekun Ma; Wu Zhang; Rui Zhang; Meng Zhang; Guangcheng Xi; Yitai Qian

doi:10.1166/jnn.2005.142

A facile hydrothermal synthesis route to single-crystalline lead iodide nanobelts and nanobelt bundles

Dekun Ma, Wu Zhang, Rui Zhang, Meng Zhang, Guangcheng Xi, Yitai Qian

Pharmaceutical Care and Health Systems

Research output: Contribution to journal › Article › peer-review

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Abstract

Single-crystalline PbI ₂ nanobelt bundles have been prepared using lead monoxide powder and hydroiodic acid as reagents at the assistance of dodecylamine. The assembled PbI ₂ nanobelt bundles can be spilt into nanobelts through long-playing sonication. The prepared nanobelt bundles consist of several nanobelts and the nanobelts have lengths of tens of microns, widths of 50-150 nanometers, and thicknesses ca. 20 nanometers. X-Ray diffraction (XRD), scanning electron microscopy (SEM), field emission scanning electron microscopy (FE-SEM) transmission electron microscopy (TEM), electronic diffraction (ED), and high-resolution transmission microscopy (HRTEM) was used to characterize the as-prepared product. The possible formation mechanism of PbI ₂ nanobelt bundles was tentatively proposed.

Original language	English (US)
Pages (from-to)	810-813
Number of pages	4
Journal	Journal of Nanoscience and Nanotechnology
Volume	5
Issue number	5
DOIs	https://doi.org/10.1166/jnn.2005.142
State	Published - 2005

Keywords

Hydrothermal synthesis
Nanobelt bundles
Nanostructures
PbI
Semiconductors

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10.1166/jnn.2005.142

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title = "A facile hydrothermal synthesis route to single-crystalline lead iodide nanobelts and nanobelt bundles",

abstract = "Single-crystalline PbI 2 nanobelt bundles have been prepared using lead monoxide powder and hydroiodic acid as reagents at the assistance of dodecylamine. The assembled PbI 2 nanobelt bundles can be spilt into nanobelts through long-playing sonication. The prepared nanobelt bundles consist of several nanobelts and the nanobelts have lengths of tens of microns, widths of 50-150 nanometers, and thicknesses ca. 20 nanometers. X-Ray diffraction (XRD), scanning electron microscopy (SEM), field emission scanning electron microscopy (FE-SEM) transmission electron microscopy (TEM), electronic diffraction (ED), and high-resolution transmission microscopy (HRTEM) was used to characterize the as-prepared product. The possible formation mechanism of PbI 2 nanobelt bundles was tentatively proposed.",

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author = "Dekun Ma and Wu Zhang and Rui Zhang and Meng Zhang and Guangcheng Xi and Yitai Qian",

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T1 - A facile hydrothermal synthesis route to single-crystalline lead iodide nanobelts and nanobelt bundles

AU - Ma, Dekun

AU - Zhang, Wu

AU - Zhang, Rui

AU - Zhang, Meng

AU - Xi, Guangcheng

AU - Qian, Yitai

PY - 2005

Y1 - 2005

N2 - Single-crystalline PbI 2 nanobelt bundles have been prepared using lead monoxide powder and hydroiodic acid as reagents at the assistance of dodecylamine. The assembled PbI 2 nanobelt bundles can be spilt into nanobelts through long-playing sonication. The prepared nanobelt bundles consist of several nanobelts and the nanobelts have lengths of tens of microns, widths of 50-150 nanometers, and thicknesses ca. 20 nanometers. X-Ray diffraction (XRD), scanning electron microscopy (SEM), field emission scanning electron microscopy (FE-SEM) transmission electron microscopy (TEM), electronic diffraction (ED), and high-resolution transmission microscopy (HRTEM) was used to characterize the as-prepared product. The possible formation mechanism of PbI 2 nanobelt bundles was tentatively proposed.

AB - Single-crystalline PbI 2 nanobelt bundles have been prepared using lead monoxide powder and hydroiodic acid as reagents at the assistance of dodecylamine. The assembled PbI 2 nanobelt bundles can be spilt into nanobelts through long-playing sonication. The prepared nanobelt bundles consist of several nanobelts and the nanobelts have lengths of tens of microns, widths of 50-150 nanometers, and thicknesses ca. 20 nanometers. X-Ray diffraction (XRD), scanning electron microscopy (SEM), field emission scanning electron microscopy (FE-SEM) transmission electron microscopy (TEM), electronic diffraction (ED), and high-resolution transmission microscopy (HRTEM) was used to characterize the as-prepared product. The possible formation mechanism of PbI 2 nanobelt bundles was tentatively proposed.

KW - Hydrothermal synthesis

KW - Nanobelt bundles

KW - Nanostructures

KW - PbI

KW - Semiconductors

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A facile hydrothermal synthesis route to single-crystalline lead iodide nanobelts and nanobelt bundles

Abstract

Keywords

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