4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses

Ufuk Kumru; Fabienne Dumoulin; Erwann Jeanneau; Fatma Yuksel; Yari Cabezas; Yunus Zorlu; Vefa Ahsen

doi:10.1007/s11224-011-9850-8

4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses

Ufuk Kumru
, Fabienne Dumoulin
, Erwann Jeanneau
, Fatma Yuksel
, Yari Cabezas
, Yunus Zorlu
, Vefa Ahsen

Biotechnology Institute

Research output: Contribution to journal › Article › peer-review

20 Scopus citations

Abstract

Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.

Original language	English (US)
Pages (from-to)	175-183
Number of pages	9
Journal	Structural Chemistry
Volume	23
Issue number	1
DOIs	https://doi.org/10.1007/s11224-011-9850-8
State	Published - Feb 2012

Bibliographical note

Funding Information:
Acknowledgments The Scientific and Technological Research Council of Turkey TUBITAK (PIA Turkey-France bilateral project Bosphorus 109M356) is gratefully acknowledged. YC thanks the long-life learning Erasmus funding.

Keywords

IR
NMR
Phthalonitrile
Single-crystal
Structural analysis
Tert-Butanethiol
Tert-Butylsulfanylphthalonitrile

Publisher link

10.1007/s11224-011-9850-8

Find It

Find It at U of M Libraries

Cite this

@article{0bfeb732a988402fab1998f38b425e2d,

title = "4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses",

abstract = "Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.",

keywords = "IR, NMR, Phthalonitrile, Single-crystal, Structural analysis, Tert-Butanethiol, Tert-Butylsulfanylphthalonitrile",

author = "Ufuk Kumru and Fabienne Dumoulin and Erwann Jeanneau and Fatma Yuksel and Yari Cabezas and Yunus Zorlu and Vefa Ahsen",

note = "Funding Information: Acknowledgments The Scientific and Technological Research Council of Turkey TUBITAK (PIA Turkey-France bilateral project Bosphorus 109M356) is gratefully acknowledged. YC thanks the long-life learning Erasmus funding.",

year = "2012",

month = feb,

doi = "10.1007/s11224-011-9850-8",

language = "English (US)",

volume = "23",

pages = "175--183",

journal = "Structural Chemistry",

issn = "1040-0400",

publisher = "Springer",

number = "1",

}

TY - JOUR

T1 - 4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles

T2 - Synthesis and comparative structural and spectroscopic analyses

AU - Kumru, Ufuk

AU - Dumoulin, Fabienne

AU - Jeanneau, Erwann

AU - Yuksel, Fatma

AU - Cabezas, Yari

AU - Zorlu, Yunus

AU - Ahsen, Vefa

N1 - Funding Information: Acknowledgments The Scientific and Technological Research Council of Turkey TUBITAK (PIA Turkey-France bilateral project Bosphorus 109M356) is gratefully acknowledged. YC thanks the long-life learning Erasmus funding.

PY - 2012/2

Y1 - 2012/2

N2 - Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.

AB - Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.

KW - IR

KW - NMR

KW - Phthalonitrile

KW - Single-crystal

KW - Structural analysis

KW - Tert-Butanethiol

KW - Tert-Butylsulfanylphthalonitrile

UR - https://www.scopus.com/pages/publications/84862661972

UR - https://www.scopus.com/pages/publications/84862661972#tab=citedBy

U2 - 10.1007/s11224-011-9850-8

DO - 10.1007/s11224-011-9850-8

M3 - Article

AN - SCOPUS:84862661972

SN - 1040-0400

VL - 23

SP - 175

EP - 183

JO - Structural Chemistry

JF - Structural Chemistry

IS - 1

ER -

4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses

Abstract

Bibliographical note

Keywords

Publisher link

Find It

Other files and links

Fingerprint

Cite this