4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses

Ufuk Kumru; Fabienne Dumoulin; Erwann Jeanneau; Fatma Yuksel; Yari Cabezas; Yunus Zorlu; Vefa Ahsen

doi:10.1007/s11224-011-9850-8

4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses

Ufuk Kumru, Fabienne Dumoulin, Erwann Jeanneau, Fatma Yuksel, Yari Cabezas, Yunus Zorlu, Vefa Ahsen

Biotechnology Institute

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20 Scopus citations

Abstract

Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.

Original language	English (US)
Pages (from-to)	175-183
Number of pages	9
Journal	Structural Chemistry
Volume	23
Issue number	1
DOIs	https://doi.org/10.1007/s11224-011-9850-8
State	Published - Feb 2012

Bibliographical note

Funding Information:
Acknowledgments The Scientific and Technological Research Council of Turkey TUBITAK (PIA Turkey-France bilateral project Bosphorus 109M356) is gratefully acknowledged. YC thanks the long-life learning Erasmus funding.

Keywords

IR
NMR
Phthalonitrile
Single-crystal
Structural analysis
Tert-Butanethiol
Tert-Butylsulfanylphthalonitrile

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10.1007/s11224-011-9850-8

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abstract = "Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.",

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AU - Kumru, Ufuk

AU - Dumoulin, Fabienne

AU - Jeanneau, Erwann

AU - Yuksel, Fatma

AU - Cabezas, Yari

AU - Zorlu, Yunus

AU - Ahsen, Vefa

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N2 - Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.

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KW - NMR

KW - Phthalonitrile

KW - Single-crystal

KW - Structural analysis

KW - Tert-Butanethiol

KW - Tert-Butylsulfanylphthalonitrile

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4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: Synthesis and comparative structural and spectroscopic analyses

Abstract

Bibliographical note

Keywords

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