Abstract
Amidobenziodoxoles 2 can be prepared from benziodoxole 1, trimethylsilyltriflate and the appropriate amides in the form of stable, microcrystalline compounds. Amidobenziodoxoles 2 react with adamantane 3 or N,N-dimethylarylamines 5 to afford the corresponding products of amidation, 4 and 6.
Original language | English (US) |
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Pages (from-to) | 21-24 |
Number of pages | 4 |
Journal | Tetrahedron Letters |
Volume | 38 |
Issue number | 1 |
DOIs | |
State | Published - Jan 6 1997 |
Bibliographical note
Funding Information:In conclusion, we have prepared and isolated as individual, stable compounds amidobenziodoxoles 2a- e. Compounds 2 are potentially useful reagents for direct amidation of adamantane and N,N- dialkylarylamines. Acknowledgement. This work was supported by a research grant from the National Science Foundation (NSF/CHE-9505868) and by the Undergraduate Research Opportunities Program at the University of Minnesota.